Andrea C

Sounds like you have a model 2450 SourceMeter.
You could use a triax shorting plug on the Force LO to connect the center pin to outer shell which is at chassis ground.
Keithley part number for shorting plug:  CS-1546
Info about CS-1546 Triax Shorting Plug

You do have the older 4200-SCS running the KITE software.
More than 10 years ago, we transitioned to 4200A-SCS and Clarius software.
Keep in mind, there is always an upgrade path.  Contact your local sales office for more information.

For repeated execution of an ITM, check out the Reference Manual on enabling the cycle mode.
I believe max number of cycles is 128.  When running the cycle mode, the ITM test results will have a tab for each cycle.
This is similar to having multiple append tabs.  But cycle mode relieves you of some button pushing.

If cycle mode is not enough cycles, you might be able to use the Stress/Measure cycling and just pick a benign stress condition.

Alternately, you could close the KITE GUI interface and instead use external command interface (KXCI).  And then from another computer you can send commands over GPIB or LAN to do the repeated IV curves and read back the data.
 

Does your SMU1 also have a 4200-PA?

In your pseudocode, you have a DV2 but no other parameters.  Is SMU2 playing a role in this setup?

If you run an ITM out of KITE for the voltage sweep on the 80KΩ, any clicking then?

Sounds like some range selection issues are going on with the clicking.
Especially if you have the 4200-PA, you could try using the RG command to exclude some of the lowest and most sensitive ranges.
Without a pre-amp, the 100nA and higher ranges are available from the SMU.

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If the instrument is busy carrying out the sweep, then the VISA write of the "*OPC?" command is not processed until the sweep completes.  This is why the VISA read will timeout.

An alternate approach is to use VISA's ReadSTB() to obtain the value of the status byte or status.condition register.

I put an elaboration and Python sample in the attached document.

Hello,
The PDF is too large for attaching, so here is link to Box:

Reference Manual for the original 2600 models

The LAN communication can be applied from your router (DHCP) or selected manually.

Sounds like you have been using DHCP and the router is periodically giving new address?

Perhaps you can reserve an address in the router setup and manually configure the instrument to use it?

Appendix B-2 in the 2400 Series User Manual has the error codes.
NOTE:  this is not the touch screen models (2450, etc).

User Manual for 2400 Series SourceMeter

Some general comments:

For switching pA levels, consider the offset current spec of the switch.

For parallel reliability testing, consider using a power supply to apply voltage bias to N devices.
And then switch in a sensitive amp meter one by one.
When not measuring the current, the switching scheme needs to maintain pathway completion for the current to flow.
Model 3761 switch is one example.

KickStart does not use tsp-link for communication with the SMU.
KickStart needs a computer connection to each SMU (lan, usb or gpib).

If you additionally have tsp-link between the instruments, KickStart can use that for their triggering/coordination.
 

The 4.x firmware of 2600B series apply only to units shipped from factory with a 4.x level.

If your 2600B has 3.x level, then 3.4.2 from Tek.com would be the most recent version.